Coordinated isotopic and TEM studies of presolar graphites from Murchison

Croat T. K., Stadermann F. J., Zinner E., and Bernatowicz T. J. (2004)
Lunar and Planetary Science XXXV, Abstract #1353, LPI Houston.


ABSTRACT

Previous microstructural (SEM) and isotopic studies of the Murchison KFC1 separate (2.15-2.20 g/ml) found many presolar graphites with an average size of 1.5 microns. Carbon isotopic ratios ranged over 3 orders of magnitude (from 0.02 to 80 times the solar value of 89). Two morphological types of presolar graphites were found, with dense "onion" graphites and less dense "cauliflower" graphites, although these types are not isotopically distinct in carbon. Further transmission electron microscope (TEM) studies of the "onion" graphites revealed numerous internal refractory carbides ((Ti,Zr,Mo,Ru)C) and also some graphites with a nanocrystalline core surrounded by a well-graphitized rim. Due to their small size, TEM analyses of graphites that had been isotopically characterized were not possible. In the present work, more graphites were examined in TEM, including the larger "cauliflower" graphites omitted from the earlier study, and isotopic analysis was performed on the same samples examined in the TEM.


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